{"id":38346,"date":"2024-03-26T16:42:35","date_gmt":"2024-03-26T16:42:35","guid":{"rendered":"https:\/\/www.alicat.com\/?post_type=article&#038;p=38346"},"modified":"2026-01-26T20:44:01","modified_gmt":"2026-01-26T20:44:01","slug":"duralar-innoviert-physikalische-aufdampf-verfahren-mit-massenstrom-steuerung","status":"publish","type":"support","link":"https:\/\/www.alicat.com\/de\/support\/duralar-innovates-physical-vapor-deposition-processes-using-mass-flow-control\/","title":{"rendered":"Duralar innoviert Verfahren zur physikalischen Gasphasenabscheidung mit Massendurchflussregelung"},"content":{"rendered":"\n[et_pb_section fb_built=&#8221;1&#8243; _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_row _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; custom_padding=&#8221;||0px|||&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_column type=&#8221;4_4&#8243; _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_text _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;]<div id=\"eckb-article-content-header\">\n<h1 class=\"eckb-article-title\"><strong>Duralar innovates physical vapor deposition processes using mass flow control<\/strong><\/h1>\n<div class=\"eckb-article-content-header__article-meta\"><\/div>\n<\/div>\n<div id=\"eckb-article-content-body\">\n<p>While anodizing and bluing prevent corrosion, it doesn\u2019t strengthen the surface much and can scratch off. Chrome plating has been an alternative, but chrome-6 is toxic, and can still wear, pit, and spall.<\/p>\n<p>Vacuum deposition system manufacturer, <a href=\"https:\/\/duralar.com\/\" target=\"_blank\" rel=\"noopener\">Duralar<\/a>, wanted to develop a fast, diamond-like coating process using physical vapor deposition that\u2019s harder and more durable than either. It would have applications in the prevention of corrosion, erosion, and wear on metal parts.<\/p>\n<\/div>[\/et_pb_text][et_pb_text _builder_version=&#8221;4.27.4&#8243; _module_preset=&#8221;default&#8221; width=&#8221;80.9%&#8221; module_alignment=&#8221;center&#8221; min_height=&#8221;361.6px&#8221; custom_margin=&#8221;20px||20px||false|false&#8221; custom_padding=&#8221;10px|20px|10px|10px|false|false&#8221; hover_enabled=&#8221;0&#8243; border_color_all=&#8221;#EAEAEA&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221; sticky_enabled=&#8221;0&#8243;]<img decoding=\"async\" src=\"https:\/\/www.alicat.com\/wp-content\/uploads\/2024\/08\/vapor-dep-sys-wild.webp\" width=\"600\" height=\"335\" alt=\"Duralar's physical vapor deposition system using Alicat Scientific instruments.\" class=\"wp-image-42083 aligncenter size-full\" srcset=\"https:\/\/www.alicat.com\/wp-content\/uploads\/2024\/08\/vapor-dep-sys-wild.webp 600w, https:\/\/www.alicat.com\/wp-content\/uploads\/2024\/08\/vapor-dep-sys-wild-480x268.webp 480w\" sizes=\"(min-width: 0px) and (max-width: 480px) 480px, (min-width: 481px) 600px, 100vw\" \/>\n<p id=\"caption-attachment-10699\" class=\"wp-caption-text\" style=\"text-align: center;\">After the diamond-hard PVD vacuum coating, plain steel shows as black.<\/p>[\/et_pb_text][\/et_pb_column][\/et_pb_row][et_pb_row _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; custom_padding=&#8221;7px|||||&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_column type=&#8221;4_4&#8243; _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_text _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;]<h2><strong>Challenge 1<\/strong>: Practical innovation requires versatile flow control<\/h2>\n<p><span>R&amp;D means testing, allowing for new formulations of barrier and reactive gases. This requires troubleshooting with different flow ratios and gas types. Duralar needed to find a way to maintain accurate, repeatable flow for changing flow ratios and gases while minimizing the need to recalibrate or purchase new controllers.<\/span><\/p>\n<p><span>They started with a generic vacuum deposition system, but none of the six built-in thermal controllers were calibrated for tetramethylsilane (TMS), a vaporized liquid. The controllers were also unable to accurately flow different gas types without recalibration.<\/span><\/p>\n<h2>Solution: Anticorrosive mass flow controller with custom gas calibration<\/h2>\n<p>TMS isn\u2019t on Alicat\u2019s <a href=\"https:\/\/www.alicat.com\/documentation\/gas-select-gas-list\/\">standard gas list<\/a>, however, our engineers were able to provide Duralar with a custom solution. The mass flow controller was built as a drop-in replacement, with <a href=\"https:\/\/www.alicat.com\/products\/gas-flow\/mass-flow-controller\/laminar-dp-mass-flow-controllers\/\" target=\"_blank\" rel=\"noopener\">corrosion resistance<\/a> and a custom TMS gas calibration.<\/p>\n<p>Because Alicat devices operate using <a href=\"https:\/\/www.alicat.com\/support\/theory-of-operation-laminar-differential-pressure-flow-measurement\/\" target=\"_blank\" rel=\"noopener\">laminar differential pressure technology<\/a>, they also provided Duralar with a few additional benefits over their old thermal controllers:<\/p>\n<ul>\n<li><span style=\"color: #000000;\">Alicat devices are preloaded with complete performance curves for all preloaded gas calibrations, enabling high-accuracy flow control from 0.5% to 100% of full scale<\/span><\/li>\n<li><span style=\"color: #000000;\">No inaccuracies due to changing temperature or pressure conditions, since the closed-loop sensor in the controller compensates for volumetric changes<\/span><\/li>\n<\/ul>\n<p>Soon, Duralar was producing coated parts by pumping down the chamber to a vacuum, flowing in just the right amount of gases, adding material vapor, and turning it into a plasma that bonds to the parts.<\/p>[\/et_pb_text][\/et_pb_column][\/et_pb_row][et_pb_row column_structure=&#8221;3_5,2_5&#8243; _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; custom_padding=&#8221;7px|||||&#8221; locked=&#8221;off&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_column type=&#8221;3_5&#8243; _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_text _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;]<h2><strong>Challenge 2<\/strong>: Developing a process to deposit thin coatings<\/h2>\n<p>Next, they wanted to develop a process to deposit this thin coating inside tubes and pipes so they could reduce abrasive wear and corrosion. The technique is clever: seal the ends of the tubes, effectively converting the interior of the tube into the vacuum chamber.<\/p>\n<p>The challenge is being able to vary the location of the plasma-producing electrical discharge inside a narrow tube to get a complete coating. To find a solution, Duralar dove again into prototyping and further experimentation.<\/p>\n<h2><\/h2>\n<h2>Solution: Two more mass flow controllers<\/h2>\n<p>By using an anticorrosive flow controller for the corrosive TMS and two additional Alicat <a href=\"https:\/\/www.alicat.com\/products\/gas-flow\/mass-flow-controller\/laminar-dp-mass-flow-controllers\/\" target=\"_blank\" rel=\"noopener\">mass flow controllers<\/a>, they were able to switch between flowing up to 130 preloaded gases and <a href=\"https:\/\/www.alicat.com\/support\/gas-select-composer-gas-mix-calibration\/\" target=\"_blank\" rel=\"noopener\">20 custom gas mixtures<\/a>.<\/p>\n<p>They also used our downloadable <a href=\"https:\/\/www.alicat.com\/documentation\/software-drivers\/\" target=\"_blank\" rel=\"noopener\">LabVIEW drivers<\/a> to build the vacuum process steps so they could control the MFCs and their shut-off solenoids from a remote laptop.<\/p>\n<h2><\/h2>\n<h2><strong>Results<\/strong><\/h2>\n<p>In due time, they had perfected the physical vapor deposition process and began building coating systems to order. Now, you can order diamond-like coatings for your metal parts\u2014or the systems to provide the service for others\u2014and the vacuum coating is more durable than anodizing, while quicker and harder than chrome plating!<\/p>[\/et_pb_text][\/et_pb_column][et_pb_column type=&#8221;2_5&#8243; _builder_version=&#8221;4.23.1&#8243; _module_preset=&#8221;default&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;][et_pb_text _builder_version=&#8221;4.27.4&#8243; _module_preset=&#8221;default&#8221; width=&#8221;75%&#8221; module_alignment=&#8221;center&#8221; custom_margin=&#8221;50px||50px||false|false&#8221; custom_padding=&#8221;20px|20px|20px|20px|false|false&#8221; border_width_all=&#8221;1px&#8221; border_color_all=&#8221;#EAEAEA&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;]<p class=\"wp-caption-text\" style=\"text-align: center;\"><img decoding=\"async\" src=\"https:\/\/www.alicat.com\/wp-content\/uploads\/2024\/08\/vapor-dep-prototype_250.webp\" width=\"250\" height=\"188\" alt=\"Before and after of diamond-hard PVD vacuum coating. Plain steel becomes black after the process.\" class=\"wp-image-42084 alignnone size-full\" \/><\/p>\n<p id=\"caption-attachment-10700\" class=\"wp-caption-text\" style=\"text-align: center;\">A vacuum pump and three mass flow controllers for prototyping.<\/p>[\/et_pb_text][et_pb_text _builder_version=&#8221;4.27.4&#8243; _module_preset=&#8221;default&#8221; width=&#8221;75%&#8221; module_alignment=&#8221;center&#8221; custom_margin=&#8221;50px||50px||false|false&#8221; custom_padding=&#8221;20px|20px|20px|20px|false|false&#8221; border_width_all=&#8221;1px&#8221; border_color_all=&#8221;#EAEAEA&#8221; global_colors_info=&#8221;{}&#8221; theme_builder_area=&#8221;post_content&#8221;]<p class=\"wp-caption-text\" style=\"text-align: center;\"><img decoding=\"async\" src=\"https:\/\/www.alicat.com\/wp-content\/uploads\/2024\/08\/holding-coated-part.webp\" width=\"800\" height=\"468\" alt=\"Vacuum pump and three mass flow controllers for prototyping.\" class=\"wp-image-42085 alignnone size-full\" srcset=\"https:\/\/www.alicat.com\/wp-content\/uploads\/2024\/08\/holding-coated-part.webp 800w, https:\/\/www.alicat.com\/wp-content\/uploads\/2024\/08\/holding-coated-part-480x281.webp 480w\" sizes=\"(min-width: 0px) and (max-width: 480px) 480px, (min-width: 481px) 800px, 100vw\" \/><\/p>\n<p id=\"caption-attachment-10700\" class=\"wp-caption-text\" style=\"text-align: center;\">After the diamond-hard PVD vacuum coating, plain steel shows as black.<\/p>[\/et_pb_text][\/et_pb_column][\/et_pb_row][\/et_pb_section]\n","protected":false},"featured_media":46458,"parent":0,"template":"","meta":{"_acf_changed":false,"_et_pb_use_builder":"on","_et_pb_old_content":"","_et_gb_content_width":"1920","content-type":"","_searchwp_excluded":""},"categories":[],"class_list":["post-38346","support","type-support","status-publish","has-post-thumbnail","hentry"],"acf":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO Premium plugin v27.6 (Yoast SEO v27.6) - 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